Al-Mu'minun 23:76

Walaqad akhathnahum bilAAathabifama istakanoo lirabbihim wama yatadarraAAoon

And We had gripped them with suffering [as a warning], but they did not yield to their Lord, nor did they humbly supplicate, [and will continue thus]

We have already seized them with punishment, but they did not turn humble to their Lord, nor do they supplicate in humility,